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The shows are restricted fans age 18 and older. He also wanted to differentiate from AKB48's usual uniforms with more sexy attire. The analyst shall ensure that samples do not become contaminated during sample preparation. Wherever possible, apparatus and equipment coming into contact with the sample shall not contain those metals to be determined and be made of inert materials e. These should be acid cleaned to minimise the risk of contamination.

High quality stainless steel may be used for cutting edges. There are many satisfactory specific sample preparation procedures which may be used for the products under consideration. In the case of inorganic tin, care shall be taken to ensure that all the material is taken into solution as losses are known to occur readily, particularly because of hydrolysis to insoluble hydrated Sn IV oxide species.

Containers shall be rinsed with high purity acetone or hexane before use to minimise the risk of contamination. Wherever possible, apparatus and equipment coming into contact with the sample shall be made of inert materials such as aluminium, glass or polished stainless steel.

Plastics such as polypropylene or PTFE shall be avoided because the analyte can adsorb onto these materials. Treatment of the sample as received in the laboratory. The complete aggregate sample shall be finely ground where relevant and thoroughly mixed using a process that has been demonstrated to achieve complete homogenisation.

The samples for enforcement, defence and referee purposes shall be taken from the homogenised material unless this conflicts with the rules of the Member States on sampling as regards the rights of the food business operator.

Repeatability the value below which the absolute difference between single test results obtained under repeatability conditions i. Standard deviation calculated from results generated under repeatability conditions. Reproducibility the value below which the absolute difference between single test results obtained under reproducibility conditions i. Limit of detection, smallest measured content, from which it is possible to deduce the presence of the analyte with reasonable statistical certainty.

Limit of quantification, lowest content of the analyte which can be measured with reasonable statistical certainty. Methods of analysis for total tin are appropriate for official control on inorganic tin levels.

Where no specific methods for the determination of contaminants in foodstuffs are prescribed at Community level, laboratories may select any validated method of analysis where possible, the validation shall include a certified reference material provided the selected method meets the specific performance criteria set out in Tables 5 to 7.

Performance criteria for methods of analysis for lead, cadmium, mercury and inorganic tin. For the latter, less than one fifth of the maximum level. For the latter, less than two fifth of the maximum level. Methods suitable for official control must produce results with standard measurement uncertainties less than the maximum standard measurement uncertainty calculated using the formula below:.

The values to be used are given in Table 8. If an extraction step is applied in the analytical method, the analytical result shall be corrected for recovery. In this case the level of recovery must be reported. In case no extraction step is applied in the analytical method e. In case the result is reported uncorrected for recovery this shall be mentioned. The present interpretation rules shall apply for the analytical result obtained on the sample for enforcement. In case of analysis for defence or reference purposes, the national rules shall apply.

Thompson, S. Ellison and R. Wood, Pure Appl. Thompson and R. Thompson, Analyst, , , Skip to main content. This document is an excerpt from the EUR-Lex website. EU case-law Case-law Digital reports Directory of case-law.

Quick search. Use quotation marks to search for an "exact phrase". Use a question mark? Search tips. Need more search options? Use the Advanced search. Document R Help Print this page. Expand all Collapse all. Title and reference. Languages, formats and link to OJ. Official Journal. Multilingual display. Article 3 This Regulation shall enter into force on the 20th day following its publication in the Official Journal of the European Union.

It shall apply from 1 June Done at Brussels, 28 March Personnel Sampling shall be performed by an authorised person as designated by the Member State.

Material to be sampled Each lot or sublot which is to be examined shall be sampled separately. Precautions to be taken In the course of sampling, precautions shall be taken to avoid any changes which would affect the levels of contaminants, adversely affect the analytical determination or make the aggregate samples unrepresentative.

Incremental samples As far as possible, incremental samples shall be taken at various places distributed throughout the lot or sublot. Preparation of the aggregate sample The aggregate sample shall be made up by combining the incremental samples. Samples for enforcement, defence and referee purposes The samples for enforcement, defence and referee purposes shall be taken from the homogenised aggregate sample unless this conflicts with the rules of the Member States as regards the rights of the food business operator.

Packaging and transmission of samples Each sample shall be placed in a clean, inert container offering adequate protection from contamination, from loss of analytes by adsorption to the internal wall of the container and against damage in transit.